Enhanced magnetic properties through tailoring of morphology of electrospun strontium hexaferrite nanofibers.
Vats. Nishtha N; Phadkule. Saket Sanjay SS; Sarma. Shrutidhara S; Negi. Devendra Singh DS; Vishal. Badri B; Vadera. Sampat Raj SR; Mishra. Durgamadhab D
Key Findings
- Calcination temperature and heating rate control the morphology of SrFe12O19 nanofibers and embedded nanoparticles
- A sample heated to 800 °C at 10 °C/min showed the best magnetic properties compared to other temperatures
- Lower temperature (422 °C) fully decomposes the polymer and forms the ferrite phase
Practical Outcomes
- There are no actionable insights for biohackers or health‑focused protocols; the results are specific to magnetic material engineering and not applicable to human health or performance.
Summary
This paper explains how changing heating temperature and speed during production tweaks the shape and magnetic strength of tiny strontium ferrite fibers, but it has no connection to health, longevity, or performance applications.
Abstract
This work reports a simple yet unique way of tailoring the morphology of M-type Strontium Hexaferrite, SrFe<sub>12</sub>O<sub>19</sub> (SFO) particles inside the nanofibers. The reported materials were synthesized by the polymer-sol-assisted electrospinning technique followed by calcination. Calcination temperature and rate of heating play significant role in controlling the morphology of SFO nanofibers in terms of shapes, size and distribution thereby having a direct bearing on the resultant magnetic properties. The synthesized materials were investigated using X-ray Diffraction (XRD), Field Emission Scanning Electron Microscopy (FESEM), High Resolution Transmission Electron Microscopy (HRTEM), Thermogravimetric-Differential Thermal Analysis (TG-DTA), and Magnetic Property Measurement System (MPMS). The XRD analysis shows formation of almost phase pure SFO with very minute quantities of secondary phase as hematite. The FESEM images show wide range of morphologies of SFO nanofibers and specifically the nanoparticles present within the nanofibers (from irregular to platelet-like shape) thereby demonstrating the tailoring of morphologies of not only of nanofibers but nanoparticles within the nanofibers simply through variations of two parameters viz. calcination temperature and rate of heating. The TG-DTA results show that complete decomposition of PVP and formation of the SFO crystallization takes place at a much lower temperature of 422 <sup>o</sup>C. The room temperature hysteresis measurement showed that the sample calcined at 800 <sup>o</sup>C at heating rate of 10 <sup>o</sup>C/min has shown enhanced magnetic properties (M<sub>s</sub>, M<sub>r</sub>, and H<sub>c</sub>) than the samples calcined at 600 <sup>o</sup>C and 950 <sup>o</sup>C. The HRTEM studies show that the variation in heating rate also yields interesting variations in morphology of nanoparticles and their arrangement within nanofibers. This research work has resulted in a unique pathway of synthesizing nanofibers with controlled and variable morphology.
Study Information
pubmed
2025
2025-07-02T00:00:00.000Z
10.1038/s41598-025-04493-4
1
34